FLAVIO COGNIGNI

PhD Graduate

PhD program:: XXXVI


advisor: Prof. Marco Rossi
co-supervisor: Ing. Francesco Biancardi

Thesis title: Unlocking the Secrets of Complex Structures through Advanced Correlative Microscopy Techniques

The long journey of correlative microscopy (CM) began in 1945 when Keith Porter conducted pioneering studies demonstrating that specific details within specimens could be observed and characterized using both light microscopy (LM) and electron microscopy (EM) with proper sample preparation. Subsequent comparative attempts followed, thanks to contributions from McDonald, Pease, Hayes, and Geissenger, culminating in the development of detailed and robust protocols leading to correlative light and electron microscopy (CLEM) by 1980, as detailed in Chapter 1. Since then, CLEM has matured significantly, benefitting from technological advancements in both LM and EM fields, including super-resolution techniques overcoming the Abbe limit and the introduction of EM tomography enabling three-dimensional structure surveys with nanometric resolution. Currently, CLEM is defined as an imaging approach that combines the strengths of LM and EM to provide crucial information in the analysis of both materials and biological specimens. CLEM allows researchers to visualize the same area of the same sample using both LM and EM. This integration can be supplemented by additional complementary investigation techniques for multiscale and multimodal characterization in terms of microstructure, morphology, function, and chemistry, as extensively discussed in Chapter 2. In this thesis, practical examples and methodologies optimization for advanced CLEM experiments are provided. The innovative approach brought by CLEM has delineated the fundamental principles of modern CM, representing a game-changing element in scientific research. The laboratory landscape is currently undergoing dynamic transformation, driven by relentless scientific progress and contemporary research demands. Both academic and industrial research fields are characterized by an insatiable thirst for more precise, comprehensive, and interdisciplinary insights into material and biological sample properties and behaviors. The increasing complexity of scientific questions necessitates a holistic, multimodal, and multiscale approach, from macrostructures down to the atomic level, across multiple characterization tools. This thesis delves into the pivotal role of CM, as a key enabling technology, for the development of new investigation workflows and protocols, exploring its versatility in addressing advanced scientific problems and revealing hidden details across multiple length scales and modalities within specimens. A detailed description of a complete and modern CM workflow is provided, offering practical suggestions and procedures for effective CM experiment design, including advanced hardware and software solutions such as artificial intelligence. In Chapters 3 and 4, the application of CM workflows based on both non-destructive and destructive characterization techniques in some of today's cutting-edge scientific research fields will be described, including electronics and semiconductors, aerospace, biodegradation of recalcitrant materials, geosciences, and cultural heritage. In Chapter 3, CM is used to explore the infiltrative and degradative ability of Fusarium oxysporum on Polyethylene terephthalate (PET) with the combined use of Deep Learning (DL) techniques. The fungal strain F2 was chosen for this study among the many isolated from soil with the aid of PET baits, as it was the one performing best in growth tests on PET and had an abundant production of the enzymes cutinases and esterases, which are heavily involved in plastic degradation. The use of non-destructive high-resolution X-ray microscopy (XRM) coupled with the state-of-art DL reconstruction algorithm, called ZEISS DeepScout, revealed that the fungal strain F2 exhibited a preferential distribution and enhanced penetration when growing in proximity to edges and corners of PET fragments, compared to planar surfaces. The fungal attack resulted in a multiphase region, with variations in morphology and composition. Indeed, this study allowed for the identification of three distinct phases constituting the sample, which, thanks to additional analyses with Raman spectroscopy and energy dispersive X-ray spectroscopy (EDX), were identified as the fungal strain, biodegraded plastic, and salt crystals. The correlative microscopy approach enabled a comprehensive understanding of the interaction between the fungal strain and the PET substrate, shedding light on degradation processes, morphological changes, and potential structural alterations. This study highlights the importance of employing advanced microscopy techniques to investigate the complex dynamics of fungal plastic degradation, contributing to our understanding of potential strategies for mitigating plastic pollution. In Chapter 4, CM workflows are applied in the electronics and semiconductors field, cultural heritage and geosciences. Failure analysis engineers presented a multiscale and multimodal CM workflow for the comprehensive characterization of copper inclusions in the epitaxial layer of Superjunction Multi-drain MOSFETs. Copper inclusions can introduce defects in the crystal lattice, leading to localized areas of high resistance or conductivity and causing issues like high leakage (IDSS) or soft breakdown voltage (BVDSS). To address these challenges, a combination of LM, XRM, FIB-SEM tomography, EDX, TEM, and EELS was applied. The multimodal approach allowed failure analysis engineers to gain insights into the morphology, topology, and chemistry of the copper inclusions across different length scales. These findings revealed the distribution and characteristics of copper segregations with different shapes and sizes, providing a comprehensive understanding of their impact on the structural level of the power MOSFETs. This approach, which can be adopted in further workflows in the field of electronics and semiconductor failure analysis and research, is instrumental in addressing and mitigating issues related to epitaxial layers in Superjunction Multi-drain MOSFETs, offering valuable insights for improving device performance and reliability in power electronics applications. In the field of cultural heritage and conservation studies, researchers adopted CM workflows and proved it to be an effective mean the push the boundaries of our understanding of ancient artifacts. Conservation scientists also emphasized the importance of an integrated approach in addressing complex issues related to metallurgy and the conservation of historical artifacts. The application of advanced techniques offered new perspectives in the field of archaeology and heritage conservation, with significant implications for understanding the interactions between metallic materials and corrosive environments over time while also elucidating new corrosion models and mechanisms. CM was applied in structural geology suggesting that at a depth range between 30 and 80 km in subduction zones the genesis and migration of fluids carrying deep energy sources can lead to supralithostatic pore-fluid pressure and trigger brittle failure in omphacite-rich, mechanically strong rock types similar to eclogite. Modeling results suggest that these CH4-H2-rich fluids can lead to brittle failure much more easily compared to water-dominated fluids, with a CH4-H2-rich fluid having a volume 70% higher than pure H2O at these conditions. Immiscibility and phase separation may have favored preferential accumulation of carbon-hydrogen fluids via hydrofracturing. Researchers proposed that talcschist and serpentinites acted as low-permeability barriers and seal horizons, thus allowing pore pressure to increase until (supra)lithostatic conditions. The research group envisaged that genesis and migration of CH4-H2-rich aqueous fluids may trigger seismic activity in subduction zones at forearc depths. These processes may play an important role in promoting the migration of deep energy sources from deep source areas towards shallower reservoirs, including the subsurface biosphere where microbial life can take advantage of them through metabolic processes. The results proposed in this thesis stand as a culmination of research and exploration activities carried out by Dr. Flavio Cognigni into the realm of correlative microscopy (CM), representing a comprehensive example of the objectives that the collaboration between academic and industrial research can achieve while also paving new directions for pushing the boundaries of our exploration capabilities.

Research products

11573/1718932 - 2024 - Combined use of 3D X-ray microscopy and correlative microscopy for chemical-physical investigation of bronze Phoenician coins
Bernabale, M.; Cognigni, F.; Contessi, S.; Proietti, A.; Mancini, C.; Spagnoli, F.; De Vito, C.; Rossi, Marco - 04d Abstract in atti di convegno
conference: 110° Congresso Nazionale SIF (Bologna)
book: 110° Congresso Nazionale SIF - (9788874381401)

11573/1710525 - 2024 - Correlative microscopy and Micro-Raman spectroscopy for enhancing the evaluation of corrosion damage in archaeological objects
Bernabale, M.; Cognigni, F.; Contessi, S.; Silvestri, S.; La Penna, G.; Spagnoli, F.; De Vito, C.; Rossi, Marco - 01a Articolo in rivista
paper: JOURNAL OF CULTURAL HERITAGE (Paris: Elsevier, cop. 1999-) pp. 500-511 - issn: 1296-2074 - wos: WOS:001240452600001 (0) - scopus: 2-s2.0-85192712898 (0)

11573/1718935 - 2024 - Investigating corrosion systems in archaeological artifacts from Motya (Sicily, Italy): A Micro-Raman Spectroscopy and Correlative Imaging approach
Bernabale, M.; Cognigni, F.; Contessi, S.; Silvestri, S.; La Penna, G.; Spagnoli, F.; De Vito, C.; Rossi, Marco - 04d Abstract in atti di convegno
conference: Congresso congiunto SGI-SIMP (Bari)
book: Geology for a sustainable management of our Planet - ()

11573/1723152 - 2024 - Correlative analysis of advanced microscopy techniques for metallography and corrosion microstructures of bronze phoenician coins
Bernabale, Martina; Cognigni, Flavio; Contessi, Silvia; Proietti, Anacleto; Mancini, Chiara; Spagnoli, Federica; Rossi, Marco; De Vito, Caterina - 01a Articolo in rivista
paper: MATERIALS CHARACTERIZATION (Elsevier Science Incorporated / NY Journals:Madison Square Station, PO Box 882:New York, NY 10159:(212)633-3730, EMAIL: usinfo-f@elsevier.com, INTERNET: http://www.elsevier.com, Fax: (212)633-3680) pp. - - issn: 1044-5803 - wos: (0) - scopus: 2-s2.0-85206181741 (0)

11573/1699803 - 2024 - Methane-hydrogen-rich fluid migration may trigger seismic failure in subduction zones at forearc depths
Giuntoli, Francesco; Menegon, Luca; Siron, Guillaume; Cognigni, Flavio; Leroux, Hugues; Compagnoni, Roberto; Rossi, Marco; Vitale Brovarone, Alberto - 01a Articolo in rivista
paper: NATURE COMMUNICATIONS (London: Nature Publishing Group-Springer Nature) pp. 480- - issn: 2041-1723 - wos: (0) - scopus: (0)

11573/1710260 - 2024 - Micro and nanostructured carbon-phenolic ablators modified by PVP addition
Paglia, Laura; Bottacchiari, Rita; Cognigni, Flavio; Cerra, Sara; Genova, Virgilio; Rossi, Marco; Fratoddi, Ilaria; Marra, Francesco; Pulci, Giovanni - 01a Articolo in rivista
paper: MATERIALS & DESIGN (- Amsterdam: Elsevier Science -Reigate : Scientific and Technical Press, 1982- -Oxford OX2 8DP United Kingdom: Butterworth Heinemann Publishers) pp. 1-12 - issn: 0264-1275 - wos: WOS:001241766500001 (1) - scopus: 2-s2.0-85192833224 (2)

11573/1724748 - 2024 - Analyzing the structure and chemical composition of an Etruscan bronze fibula from Tomb Number 129 at Vulci (VT, Italy) through a non-destructive multi-analytical approach
Porcaro, M.; Cognigni, F.; La Penna, G.; Proietti, A.; Regoli, Carlo.; Casi, Carlo.; Carosi, S.; Rossi, Marco; Brunetti, Antonio.; De Vito, C. - 04d Abstract in atti di convegno
conference: Congresso congiunto SGI-SIMP (Bari)
book: Geology for a sustainable management of our Planet - ()

11573/1713032 - 2024 - Chitosan-Coated Fosetyl-Al Nanocrystals efficacy on Nicotiana tabacum colonized by Xylella fastidiosa
Tatulli, Giuseppe; Baldassarre, Francesca; Schiavi, Daniele; Tacconi, Stefano; Cognigni, Flavio; Costantini, Francesca; Balestra, Giorgio Mariano; Dini, Luciana; Pucci, Nicoletta; Rossi, Marco; Scala, Valeria; Ciccarella, Giuseppe; Loreti, Stefania - 01a Articolo in rivista
paper: PHYTOPATHOLOGY (American Phytopathological Society:3340 Pilot Knob Road:St. Paul, MN 55121:(800)328-7560, (612)454-7250, EMAIL: aps@scisoc.org, INTERNET: http://www.scisoc.org, Fax: (612)454-0766) pp. - - issn: 0031-949X - wos: (0) - scopus: (0)

11573/1722220 - 2024 - Comparing semi-automatic and deep learning-driven segmentation of an archaeological human mandible from Isola Sacra (Fiumicino, Italy, 1st - 3rd century CE)
Trocchi, Martina; Cognigni, Flavio; Galbusera, Alessia; Rossi, Marco; Sperduti, Alessandra; Mazur, Marta; Nava, Alessia; Bondioli, Luca - 04b Atto di convegno in volume
conference: 2024 IEEE International Conference on Metrology for Archaeology and Cultural Heritage (MetroArcheao2024) (La Valletta, Malta)
book: Proceedings of 2024 IEEE International Conference On Metrology For Archaeology And Cultural Heritage - ()

11573/1719105 - 2024 - Virtual histology based on 3D X-ray microscopy imaging for non-destructive age-at-death estimation of incinerated teeth from the Tophet of Motya (Sicily, 6th century BC)
Trocchi, Martina; Fattore, Luciano; Cognigni, Flavio; Cappella, Federico; Capuani, Silvia; Rossi, Marco; Manzi, Giorgio; Spagnoli, Federica - 01a Articolo in rivista
paper: ACTA IMEKO (sl: International Measurement Confederation (IMEKO)) pp. 1-10 - issn: 2221-870X - wos: (0) - scopus: (0)

11573/1717687 - 2024 - Multimodal Exploration of Ancient Teeth Dentin Microanatomy Using Traditional and High-Resolution Imaging Techniques
Trocchi, Martina; Galbusera, Alessia; Cognigni, Flavio; Bondioli, Luca; Coppa, Alfredo; Rossi, Marco; Nava, Alessia; Capuani, Silvia - 04d Abstract in atti di convegno
conference: 30th EAA Annual Meeting 2024 (Sapienza University of Rome)
book: Abstract book of 30th EAA Annual Meeting in Rome, Italy, 28th-31st August 2024 - (978-80-88441-08-3)

11573/1691309 - 2023 - Analysis of Roman Era archaeological finds from Museo Territoriale del Lago di Bolsena with non-destructive investigation techniques
Alemanno, Valentina; Atanasio, Pierfrancesco; La Penna, Giancarlo; Mancini, Chiara; Cognigni, Flavio; Silvestri, Serena; Proietti, Anacleto; Rossi, Marco; Ciccola, Alessandro; Nucara, Alessandro; Barbaro, Barbara; Binaco, Paolo; Dini, Danilo - 04b Atto di convegno in volume
conference: MetroArchaeo - 2023 IMEKO INTERNATIONAL CONFERENCE ON Metrology for Archaeology and Cultural Heritage (Roma)
book: 2023 IMEKO International conference on metrology for archaelogy and cultural heritage. Metro archaeo - (9789299009062)

11573/1700497 - 2023 - Analysis of Roman era archaeological finds from Museo Territoriale del Lago di Bolsena with non-destructive investigation techniques
Alemanno, Valentina; Atanasio, Pierfrancesco; La Penna, Giancarlo; Mancini, Chiara; Cognigni, Flavio; Silvestri, Serena; Proietti, Anacleto; Rossi, Marco; Ciccola, Alessandro; Nucara, Alessandro; Barbaro, Barbara; Binaco, Paolo; Dini, Danilo - 04b Atto di convegno in volume
conference: International Conference on Metrology for Archaeology and Cultural Heritage (Rome, Italy)
book: Proceedings - IMEKO TC4 International Conference on Metrology for Archaeology and Cultural Heritage - (978-92-990090-6-2)

11573/1689187 - 2023 - Preservation and Reproduction of an Ancient Human Humerus through X-ray Microscopy and 3D Printing
Alemanno, Valentina; Cognigni, Flavio; Fattore, Luciano; Stornelli, Eleonora; Genchi, Francesco; Rossi, Marco - 04f Poster
conference: Nanoinnovation 2023 (Università degli studi di Roma "La Sapienza" - Sede di Ingegneria "San Pietro in Vincoli")
book: Nanoinnovation 2023: book of abstract, poster session - ()

11573/1664683 - 2023 - 3D imaging of micro-segregation and corrosion behavior of alloying elements in archaeological artefacts from Motya (Sicily, Italy)
Bernabale, M.; Cognigni, F.; Mura, F.; Nigro, L.; Montanari, D.; Rossi, Marco; De Vito, C. - 01a Articolo in rivista
paper: CORROSION SCIENCE (Elsevier Science Limited:Oxford Fulfillment Center, PO Box 800, Kidlington Oxford OX5 1DX United Kingdom:011 44 1865 843000, 011 44 1865 843699, EMAIL: asianfo@elsevier.com, tcb@elsevier.co.UK, INTERNET: http://www.elsevier.com, http://www.elsevier.com/locate/shpsa/, Fax: 011 44 1865 843010) pp. - - issn: 0010-938X - wos: WOS:000904315500002 (7) - scopus: 2-s2.0-85144042764 (13)

11573/1688906 - 2023 - Multiscale characterization of corrosion in archaeological artefacts from Motya (Sicily, Italy) through X-ray microscopy
Bernabale, M.; Cognigni, F.; Rossi, Marco; De Vito, Caterina - 04d Abstract in atti di convegno
conference: The Geoscience paradigm: Resources, Risks and future perspectives, congresso congiunto SIMP, SGI, SOGEI, AIV (Potenza; Italy)
book: Abstract Book del Congresso SIMP-SGI-SOGEI-AIV - ()

11573/1684356 - 2023 - 3D fractures analysis and conservation assessment of wrought iron javelin through advanced non-invasive techniques
Bernabale, Martina; Cognigni, Flavio; Mancini, Chiara; Proietti, Anacleto; Mura, Francesco; Montanari, Daria; Nigro, Lorenzo; Rossi, Marco; De Vito, Caterina - 01a Articolo in rivista
paper: SCIENTIFIC REPORTS (London: Springer Nature London: Nature Publishing Group) pp. 1-11 - issn: 2045-2322 - wos: WOS:001018507300012 (3) - scopus: 2-s2.0-85162940767 (5)

11573/1681151 - 2023 - Evaluation of stress corrosion and micro-segregation in copper-based artefacts through X-ray Microscopy
Bernabale, Martina; Cognigni, Flavio; Medeghini, Laura; Rossi, Marco; De Vito, Caterina - 04d Abstract in atti di convegno
conference: XII Congresso Nazionale AIAr (Messina, Italia)
book: XII Congresso Nazionale AIAr - ()

11573/1687107 - 2023 - X-Ray Microscopy: A Non-Destructive Multi-Scale Imaging to Study the Inner Workings of Batteries
Cognigni, F.; Pasquali, M.; Prosini, P. P.; Paoletti, C.; Aurora, A.; Scaramuzzo, F. A.; Rossi, Marco - 01a Articolo in rivista
paper: CHEMELECTROCHEM (Weinheim: Wiley-VCH) pp. - - issn: 2196-0216 - wos: WOS:000924779100001 (3) - scopus: 2-s2.0-85151455818 (7)

11573/1689176 - 2023 - Preservation and reproduction of an ancient human humerus through x-ray microscopy and 3D printing
Cognigni, Flavio; Alemanno, Valentina; Fattore, Luciano; Stornelli, Eleonora; Genchi, Francesco; Rossi, Marco - 01a Articolo in rivista
paper: JOURNAL OF PHYSICS. CONFERENCE SERIES (Bristol : Institute of Physics Publishing) pp. 1-10 - issn: 1742-6588 - wos: (0) - scopus: 2-s2.0-85173058230 (0)

11573/1697306 - 2023 - Correlative light and electron microscopy (CLEM): a multifaceted tool for the study of geological specimens
Cognigni, Flavio; Miraglia, Lucia; Contessi, Silvia; Biancardi, Francesco; Rossi, Marco - 01a Articolo in rivista
paper: JOURNAL OF EXPERIMENTAL AND THEORETICAL ANALYSES (Basel Switzerland: MDPI) pp. 74-85 - issn: 2813-4648 - wos: (0) - scopus: (0)

11573/1686307 - 2023 - X‐ray microscopy. A non‐destructive multi‐scale imaging to study the inner workings of batteries
Cognigni, Flavio; Pasquali, Mauro; Prosini, Pier Paolo; Paoletti, Claudia; Aurora, Annalisa; Scaramuzzo, Francesca Anna; Rossi, Marco - 01a Articolo in rivista
paper: CHEMELECTROCHEM (Weinheim: Wiley-VCH) pp. 1-9 - issn: 2196-0216 - wos: WOS:000924779100001 (3) - scopus: 2-s2.0-85151455818 (7)

11573/1697304 - 2023 - A multiscale and multimodal correlative microscopy workflow to characterize copper segregations identified in epitaxial layer of power MOSFETs
Cognigni, Flavio; Rossi, Marco; Stegmann, Heiko; Sciuto, Giuseppe; Anastasi, Giuseppe; Astuto, Massimiliano; Bonadonna, Marco; Mello, Domenico - 04b Atto di convegno in volume
conference: International Symposium for Testing and Failure Analysis (Phoenix, Arizona, USA)
book: ISTFA Proceedings - ()

11573/1686446 - 2023 - Multimodal and multiscale investigation for the optimization of AlSi10Mg components made by powder bed fusion-laser beam
Cognigni, Flavio; Sgambetterra, Mirko; Zucca, Guido; Gentile, Domenico; Ricci, Sara; Testa, Gabriel; Rizzi, Gabriele; Rossi, Marco - 01a Articolo in rivista
paper: DISCOVER MATERIALS (Cham: Springer International Publishing) pp. - - issn: 2730-7727 - wos: (0) - scopus: 2-s2.0-85190138383 (1)

11573/1707570 - 2023 - Exploring the infiltrative and degradative ability of Fusarium oxysporum on polyethylene terephthalate (PET) using correlative microscopy and deep learning
Cognigni, Flavio; Temporiti, Marta Eleonora Elisabetta.; Nicola, Lidia; Gueninchault, Nicolas; Tosi, Solveig; Rossi, Marco - 01a Articolo in rivista
paper: SCIENTIFIC REPORTS (London: Springer Nature London: Nature Publishing Group) pp. - - issn: 2045-2322 - wos: WOS:001133375600029 (1) - scopus: 2-s2.0-85180704035 (2)

11573/1685959 - 2023 - Low-velocity impact behaviour of biocomposite laminates reinforced by flax, basalt and hybrid fibres at various temperatures: analytical, numerical and experimental results
Giammaria, V.; Boria, S.; Sarasini, F.; Tirillo', J.; Cognigni, F.; Rossi, M.; Fischer, B.; Pornbacher, J. - 01a Articolo in rivista
paper: COMPOSITE STRUCTURES (-OXFORD, ENGLAND: Elsevier Science Ltd -London : Applied Science, 1983-) pp. - - issn: 0263-8223 - wos: WOS:001047471900001 (5) - scopus: 2-s2.0-85165536705 (6)

11573/1682333 - 2023 - The role of the Moonmilk speleothem in hypogeal archaeological sites
Kratter, Matilde; Benedetti, Francesca; Cirigliano, Angela; Cristina Tomassetti, Maria; Bellelli, Vincenzo; Rosangela Dellù, Elena; Sivilli, Sandra; Mura, Francesco; Cognigni, Flavio; Rossi, Marco; Ingallina, Cinzia; Mannina, Luisa; Ronca, Sara; Brandano, Marco; Quagliariello, Andrea; Rinaldi, Teresa - 04f Poster
conference: XXI INQUA Congress 2023 (Rome, Italy)
book: XXI INQUA Congress 2023 - Abstract book - ()

11573/1697316 - 2023 - Advances in focused ion beam tomography for three-dimensional characterization in materials science
Mura, Francesco; Cognigni, Flavio; Ferroni, Matteo; Morandi, Vittorio; Rossi, Marco - 01a Articolo in rivista
paper: MATERIALS (Basel: Molecular Diversity Preservation International-MDPI) pp. - - issn: 1996-1944 - wos: WOS:001061268400001 (3) - scopus: (0)

11573/1690586 - 2023 - XRM imaging for non-destructive age at death estimation of the incinerated teeth from the Motya Tophet (Sicily, 6th century BC)
Trocchi, Martina; Fattore, Luciano; Cognigni, Flavio; Cappella, Federico; Rossi, Marco; Manzi, Giorgio; Nigro, Lorenzo - 04b Atto di convegno in volume
conference: 2023 IMEKO TC-4 International Conference on Metrology for Archaeology and Cultural Heritage MetroArchaeo (Roma Tre University, Rome)
book: Proceedings of IMEKO TC-4 2023 International Conference on Metrology for Archaeology and Cultural Heritage MetroArchaeo - (9781713888345)

11573/1645138 - 2022 - A comprehensive strategy for exploring corrosion in iron-based artefacts through advanced Multiscale X-ray Microscopy
Bernabale, Martina; Cognigni, Flavio; Nigro, Lorenzo; Rossi, Marco; De Caro, Tilde; De Vito, Caterina - 01a Articolo in rivista
paper: SCIENTIFIC REPORTS (London: Springer Nature London: Nature Publishing Group) pp. 1-9 - issn: 2045-2322 - wos: WOS:000782202600028 (11) - scopus: 2-s2.0-85128159644 (14)

11573/1676845 - 2022 - Conventional and advanced techniques for archaeological diagnostic of iron artefacts
Bernabale, Martina; Cognigni, Flavio; Nigro, Lorenzo; Rossi, Marco; De Vito, Caterina - 04b Atto di convegno in volume
conference: 2022 IMEKO TC-4 International Conference on Metrology for Archaeology and Cultural Heritage, MetroArchaeo 2022 (Cosenza, Italia)
book: 2022 IMEKO TC-4 International Conference on Metrology for Archaeology and Cultural Heritage, MetroArchaeo 2022 - (9781713867982)

11573/1664687 - 2022 - 3D X-ray microscopy (XRM) investigation of exogenous materials inside mussels’ organs
Cognigni, F; Dinarelli, S; Girasole, M; Longo, G; Fabi, G; Rossi, Marco - 04c Atto di convegno in rivista
paper: IOP CONFERENCE SERIES: MATERIALS SCIENCE AND ENGINEERING (IOP electronic journals) pp. 012012- - issn: 1757-8981 - wos: (0) - scopus: (0)
conference: Nanoinnovation 2021 (Sapienza Università di Roma)

11573/1664690 - 2022 - X-ray microscopy – A non-destructive high-resolution imaging to study the inner workings of batteries
Cognigni, Flavio; Pasquali, Mauro; Prosini, Pier Paolo; Paoletti, Claudia; Aurora, Annalisa; Rossi, Marco - 04d Abstract in atti di convegno
conference: Giornate dell'Elettrochimica Italiana (GEI) 2022 (Orvieto (TR))
book: GEI 2022 - Collection of abstracts - ()

11573/1697312 - 2022 - Hydrocarbon-bearing fluid migration produces brecciation at high pressure condition in subduction
Giuntoli, Francesco; Vitale Brovarone, Alberto; Menegon, Luca; Siron, Guillaume; Cognigni, Flavio; Rossi, Marco - 04f Poster
conference: Congresso SGI-SIMP 2022 - Geosciences for a sustainable future (Turin, Italy)
book: Società Geologica Italiana - ()

11573/1664686 - 2022 - New approach in physical failure analysis based on 3D reconstruction
Mello, Domenico; Sciuto, Giuseppe; Astuto, Massimiliano; Francesca Santangelo, M.; Stegmann, Heiko; Cognigni, Flavio; Rossi, Marco - 04b Atto di convegno in volume
conference: International Symposium for Testing and Failure Analysis (ISTFA) 2022 (Pasadena, California, USA)
book: ISTFA 2022: Conference Proceedings from the 48th International Symposium for Testing and Failure Analysis - ()

11573/1604535 - 2021 - Review - multiscale characterization of Li-Ion batteries through the combined use of atomic force microscopy and X-ray microscopy and considerations for a correlative analysis of the reviewed data
Dini, D.; Cognigni, F.; Passeri, D.; Scaramuzzo, F. A.; Pasquali, M.; Rossi, Marco - 01a Articolo in rivista
paper: JOURNAL OF THE ELECTROCHEMICAL SOCIETY (Electrochemical Society:65 South Main Street, Building D:Pennington, NJ 08534:(609)737-1902, EMAIL: ecs@electrochem.org, orders@electrochem.org, INTERNET: http://www.electrochem.org, Fax: (609)737-2743) pp. 1-19 - issn: 0013-4651 - wos: WOS:000734052300001 (10) - scopus: 2-s2.0-85122570789 (9)

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